HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 14650083, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | Ammonium Bicarbonate | HCID 14013 | — |
| Reactant | 2-Propionylthiophene | HCID 26179 | — |
| Product | HCID 14650083 | HCID 14650083 | — |
Reaction Steps
A mixture of 2-propionylthiophene (50 g), sodium cyanide (19.9 g), ammonium bicarbonate (106 g) and an aqueous methanol solution is stirred for 5 hours under increased pressure with heating. After cooling, the precipitates are collected by filtration, washed and dried, whereby 5-ethyl-5-(2-thienyl)hydantoin (45 g) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857543 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-74becec1bfa84b4e9bd0d9ac4bb470fc |
| Source note | uspto-grants-1989_08 |