HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14989152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Penten-3-one | HCID 15394 | — |
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 14989152 | HCID 14989152 | — |
Reaction Steps
The title compound of Example 2 (5.0 g, 0.021 mole) was reacted with ethylvinyl ketone (6.3 ml) and triethylamine (1 ml) in methanol (30 ml) by the method of Example 3 to give the title compound, m.p. ca. 76°-79° C. Analysis calc. for C19H30O2S(332.50):
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857558 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-19527d7f08ec4eb29bafb4f3990624b7 |
| Source note | uspto-grants-1989_08 |