HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxycarbonyl-2-(1-naphthylmethylene)propionic acid → 3-Methoxycarbonyl-2-(1-naphthylmethyl)propionic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxycarbonyl-2-(1-naphthylmethylene)propionic acid | HCID 54382754 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Methoxycarbonyl-2-(1-naphthylmethyl)propionic acid | HCID 14095362 | 98.9% |
Reaction Steps
To a solution of 251 mg of the propionic acid compound in 10 ml of methyl alcohol was added 30 mg of a 10% palladium charcoal, and the mixture was hydrogenated under a hydrogen atmosphere at room temperature. After filtration of the catalyst, the reaction mixture was concentrated under reduced pressure to obtain 250 mg of 3-methoxycarbonyl-2-(1-naphthylmethyl)propionic acid as a white powder.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857650 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-688cffc0842f42babee884432e3272df |
| Source note | uspto-grants-1989_08 |