HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → 2,4(1H,3H)-Pyrimidinedione, 3-(4-chloro-5-ethoxy-2-fluorophenyl)-1-methyl-6-(trifluoromethyl)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | HCID 20025910 | HCID 20025910 | — |
| Product | 2,4(1H,3H)-Pyrimidinedione, 3-(4-chloro-5-ethoxy-2-fluorophenyl)-1-methyl-6-(trifluoromethyl)- | HCID 135398 | — |
Reaction Steps
using 3-(5-ethoxy-4-chloro-2-fluorophenyl)-6-trifluoromethyl- 2,4(1H,3H)-pyrimidinedione and dimethyl sulphate there is obtained 3-(5-ethoxy-4-chloro-2-fluorophenyl)-1-methyl-6 -trifluoromethyl-2,4(1H,3H)-pyrimidinedione, m.p. 118°-121° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04859229 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-b444889118394297863ec29961bea310 |
| Source note | uspto-grants-1989_08 |