Dimethyl Sulfate → HCID 15906747, compound

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using ethyl 2-[2-chloro-5-(3,6-dihydro-2,6-dioxo-4-trifluoromethyl-1(2H)-pyrimidinyl)-4-fluorophenoxy]-propionate and dimethyl sulphate there is obtained ethyl 2-[2-chloro-5-(3,6-dihydro-2,6-dioxo-3-methyl-4-trifluoromethyl-1(2H)-pyrimidinyl)-4-fluorophenoxy]-propionate, 1H-NMR (CDCl3, 400 MHz): 7.32 ppm (d,1H), 6.83 ppm (d,0.5H), 6.81 ppm (d,0.5H), 6.34 ppm (2s,1H), 4.53-4.72 ppm (m,1H), 4.13-4.27 ppm (m,2H), 3.50-3.59 ppm (m,3H), 1.67 ppm (d,3H), 1.18-1.28 ppm (m.3H):

Provenance & Evidence