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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1722948Generated: October 31, 2026

Dimethyl Sulfate → HCID 20026051, compound

https://huagongshe.com/reaction/1722948

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethyl SulfateHCID 6497—
ReactantSodium BicarbonateHCID 516892—
ReactantHCID 20026095HCID 20026095—
SolventAcetoneHCID 180—
ProductHCID 20026051HCID 20026051—

Reaction Steps

using 3-(4-chloro-2-fluoro-5-isopropoxyphenyl)-5-fluoro-6-pentafluoroethyl-2,4(1H,3H)-pyrimidinedione in acetone with sodium bicarbonate and dimethyl sulphate there is obtained 3-(4-chloro-2-fluoro-5-isopropoxyphenyl)-5-fluoro-1-methyl-6-pentafluoroethyl-2,4(1H,3H)-pyrimidinedione, m.p. 107°-109° C.;

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04859229
Source datasetuspto-grants-1989_08
ORD IDord-b6147a10054048c889e5316bdd96c8d4
Source noteuspto-grants-1989_08