Sodium Carbonate → HCID 20026075, compound

Participants

Reaction Steps

using 3-(4-chloro-2-fluoro-5-hydroxyphenyl)-1-methyl-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione with 3-phenylpropyl bromide and sodium carbonate in dimethylformamide there is obtained 3-[4-chloro-2-fluoro-5-(3-phenylpropoxy)-phenyl]-1-methyl-6 -trifluoromethyl-2,4(1H,3H)-pyrimidinedione, 1H-NMR (CDCl3, 400 MHZ): 7.15°-7.34 ppm (m,6H), 6.71 ppm (d,1H), 6.36 ppm (s,1H), 3.96 ppm (t,2H), 3.55 ppm (d,3H), 2.83 ppm (t,2H), 2.10°-2.20 ppm (m,2H):

Provenance & Evidence