HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 70394916, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | (Isocyanatomethyl)cyclohexane | HCID 3414518 | — |
| Reactant | 1-methyl-6-trifluoromethyl-3-(4-chloro-2-fluoro-5-hydroxyphenyl)-2,4(1H,3H)-pyrimidinedione | HCID 11267757 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 70394916 | HCID 70394916 | — |
Reaction Steps
using 3-(4-chloro-2-fluoro-5-hydroxyphenyl)-1-methyl-6-trifluoromethyl-2,4(1H,3H)-pyrimidinedione with cyclohexylmethyl isocyanate and triethylamine in methylene chloride there is obtained 2-chloro-5-[3,6-dihydro-2,6-dioxo-3-methyl-4-trifluoromethyl-1(2H) -pyrimidinyl]-4-fluorophenyl cyclohexylmethylcarbamate, m.p. 132°-135° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04859229 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-83e296648cdb487697e93da258625301 |
| Source note | uspto-grants-1989_08 |