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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1722980Generated: October 30, 2026

2-Butenoic acid, 3-amino-, ethyl ester, (2Z)- → HCID 20026086, compound

https://huagongshe.com/reaction/1722980

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Butenoic acid, 3-amino-, ethyl ester, (2Z)-HCID 643756—
ReactantEthyl (4-chloro-2-fluorophenyl)carbamateHCID 887936—
ProductHCID 20026086HCID 20026086—

Reaction Steps

In an analogous manner, starting from ethyl 4-chloro-2-fluorocarbanilate and ethyl 3-aminocrotonate there is obtained 3-(4-chloro-2-fluorophenyl)-6-methyl-2,4(1H,3H) -pyrimidinedione. m.p. >220° C.; mass spectrum (m/e): 254 (M+), 235, 219, 17, 143, 108, 83, 68, 42;

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04859229
Source datasetuspto-grants-1989_08
ORD IDord-2338bd8a9fc74c608c918f4b555ff498
Source noteuspto-grants-1989_08