Hydrogen Peroxide → N-chloroacetamidomethyl acrylamide N,N-dimethyl acrylamide

HRID 1722991Notes

Reaction equation

HRID 1722991 reaction equation
[Cl:1][CH2:2][C:3]([NH:5][CH2:6][NH:7][C:8](=[O:11])[CH:9]=[CH2:10])=[O:4].[CH3:12][N:13]([CH3:18])[C:14](=[O:17])[CH:15]=[CH2:16].OO>CO>[Cl:1][CH2:2][C:3]([NH:5][CH2:6][NH:7][C:8](=[O:11])[CH:9]=[CH2:10])=[O:4].[CH3:12][N:13]([CH3:18])[C:14](=[O:17])[CH:15]=[CH2:16]

Participants

5

Reactant 3

HCID 784Hydrogen PeroxideHCID 17587N,N-DimethylacrylamideHCID 86205169N-chloroacetamidomethyl acrylamide

Product 1

HCID 86743307N-chloroacetamidomethyl acrylamide N,N-dimethyl acrylamide

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

21 g of N-chloroacetamidomethyl acrylamide, 14 g of N,N-dimethyl acrylamide, 850 g of methanol and 42 ml of a 33% hydrogen peroxide solution are placed in a Hanovia-type photochemical reactor equipped with a 100 W medium pressure lamp.

Workup

  1. customequipped with a 100 W medium pressure lamp

Sources & evidence

ORD record
ord-8eb33ae761e542dea811c1a498a16a70
Source dataset
uspto-grants-1989_08
Patent number
US04859460

Reaction notes

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