Propylamine → HCID 14518384, compound

HRID 1723092Notes

Reaction equation

HRID 1723092 reaction equation
Cl[C:2]1[CH:9]=[CH:8][C:5]([CH:6]=O)=[CH:4][C:3]=1[N+:10]([O-:12])=[O:11].[CH2:13]([NH2:16])[CH2:14][CH3:15]>>[N+:10]([C:3]1[CH:4]=[C:5]([CH:6]=[N:16][CH2:13][CH2:14][CH3:15])[CH:8]=[CH:9][C:2]=1[NH:10][CH2:3][CH2:2][CH3:9])([O-:12])=[O:11]

Participants

3

Reactant 2

HCID 7852PropylamineHCID 855054-Chloro-3-nitrobenzaldehyde

Product 1

HCID 14518384HCID 14518384, compound

Procedure

(a-1) A solution of 40 parts of 4-chloro-3-nitrobenzaldehyde and 338 parts of 1-propanamine was stirred and refluxed for 1.50 hour. The reaction mixture was evaporqted, yielding 53.7 parts of 2-nitro-N-propyl-4-[(propylimino)methyl]benzenamine as a residue (int. 1).

Workup

  1. temperaturerefluxed for 1.50 hour

Sources & evidence

ORD record
ord-5ff1d6d7f5db4b7da15e71ba1749b493
Source dataset
uspto-grants-1989_08
Patent number
US04859684

Reaction notes

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