HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 20026754, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | HCID 20026735 | HCID 20026735 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 20026754 | HCID 20026754 | — |
Reaction Steps
The above thiophene (2.0 g) in 10 ml of 6M HCl is heated at 80° for 33 hours. Ethanol is added, and the solvent and water are then removed. Ether is added to the residue, the suspension is filtered and the final solid is rinsed with ether to give 2-amino-4-methyl-5-(4-chlorophenyl)thiophene hydrochloric acid salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04859699 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-02f24a18563c4bd9bf413aace7aa776d |
| Source note | uspto-grants-1989_08 |