2-Chloro-1-methylpyridinium iodide → HCID 20026806, compound

HRID 1723253Notes

Reaction equation

HRID 1723253 reaction equation
[CH2:1]([NH:4][C:5]([NH:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)=S)[CH:2]=[CH2:3].[I-].ClC1C=CC=C[N+]=1C>C(N(CC)CC)C>[CH2:1]([N:4]=[C:5]=[N:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][CH:9]=1)[CH:2]=[CH2:3]

Participants

4

Reactant 2

HCID 1670692-Chloro-1-methylpyridinium iodideHCID 1549745Urea, 1-allyl-3-phenyl-2-thio-

Product 1

HCID 20026806HCID 20026806, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

0.77 g of N-allyl-N'-phenylthiourea, 0.97 g of triethylamine und 1.2 g of 2-chloro-1-methylpyridinium iodide are reacted and worked up as described in Example 4. The product is obtained as a pale yellow oil.

Workup

  1. customThe product is obtained as a pale yellow oil

Sources & evidence

ORD record
ord-6c225f9404914807ba4d9fe13a8ec4b6
Source dataset
uspto-grants-1989_08
Patent number
US04859761

Reaction notes

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