HRID1723254

反应详情

EQUATION

反应方程式

HRID 1723254 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 0.7 g N,N'-bis(allyl)carbodiimide in 10 ml of 1,2-dichloroethane is reacted with 0.27 g of cyanamide and the reaction mixture is worked up as described in Example 4. Recrystallisation from diethyl ether yields a crystalline product which melts at 66.5°-67.0° C.

WORKUP

后处理

  1. customRecrystallisation from diethyl ether
  2. customyields a crystalline product which melts at 66.5°-67.0° C.