Cyanamide → HCID 178457555, compound

HRID 1723254Notes

Reaction equation

HRID 1723254 reaction equation
[CH2:1]([N:4]=[C:5]=[N:6][CH2:7][CH:8]=[CH2:9])[CH:2]=[CH2:3].[N:10]#[C:11][NH2:12]>ClCCCl>[CH2:1]([NH:4][C:5]([NH:6][CH2:7][CH:8]=[CH2:9])=[N:12][C:11]#[N:10])[CH:2]=[CH2:3]

Participants

4

Reactant 2

HCID 9864CyanamideHCID 13428060N,N'-bis(allyl)carbodiimide

Product 1

HCID 178457555HCID 178457555, compound

Reagents, catalysts & solvents 1

HCID 111,2-DichloroethaneSolvent

Procedure

A solution of 0.7 g N,N'-bis(allyl)carbodiimide in 10 ml of 1,2-dichloroethane is reacted with 0.27 g of cyanamide and the reaction mixture is worked up as described in Example 4. Recrystallisation from diethyl ether yields a crystalline product which melts at 66.5°-67.0° C.

Workup

  1. customRecrystallisation from diethyl ether
  2. customyields a crystalline product which melts at 66.5°-67.0° C.

Sources & evidence

ORD record
ord-12df062b51ef422d8b10c2689d1996bf
Source dataset
uspto-grants-1989_08
Patent number
US04859761

Reaction notes

Loading…