HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → N,N'-bis(allyl)carbodiimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 2-Chloro-1-methylpyridinium iodide | HCID 167069 | — |
| Reactant | Thiourea, N,N'-di-2-propen-1-yl- | HCID 3034186 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | N,N'-bis(allyl)carbodiimide | HCID 13428060 | — |
Reaction Steps
1.56 g of N,N'-bis(allyl)thiourea, 2.4 g of triethylamine and 3.07 g of 2-chloro-1-methylpyridinium iodide are reacted in 40 ml of acetonitrile and the reaction mixture is worked up as described in Example 4. The product is obtained as a faintly yellowish oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04859761 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-b1e719b11ff545e7ba7de4d2f9e2dd6e |
| Source note | uspto-grants-1989_08 |