Triethylamine → N,N'-bis(allyl)carbodiimide

HRID 1723255Notes

Reaction equation

HRID 1723255 reaction equation
[CH2:1]([NH:4][C:5]([NH:7][CH2:8][CH:9]=[CH2:10])=S)[CH:2]=[CH2:3].C(N(CC)CC)C.[I-].ClC1C=CC=C[N+]=1C>C(#N)C>[CH2:1]([N:4]=[C:5]=[N:7][CH2:8][CH:9]=[CH2:10])[CH:2]=[CH2:3]

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 1670692-Chloro-1-methylpyridinium iodideHCID 3034186Thiourea, N,N'-di-2-propen-1-yl-

Product 1

HCID 13428060N,N'-bis(allyl)carbodiimide

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

1.56 g of N,N'-bis(allyl)thiourea, 2.4 g of triethylamine and 3.07 g of 2-chloro-1-methylpyridinium iodide are reacted in 40 ml of acetonitrile and the reaction mixture is worked up as described in Example 4. The product is obtained as a faintly yellowish oil.

Workup

  1. customThe product is obtained as a faintly yellowish oil

Sources & evidence

ORD record
ord-b1e719b11ff545e7ba7de4d2f9e2dd6e
Source dataset
uspto-grants-1989_08
Patent number
US04859761

Reaction notes

Loading…