HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Bromide → HCID 11244270, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Bromide | HCID 6323 | — |
| Reactant | HCID 11806499 | HCID 11806499 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 11244270 | HCID 11244270 | — |
Reaction Steps
The crude pyridine (5.95 g) was treated with methyl bromide (2.2 ml) in acetone (25 ml). After heating in a sealed vessel at 53° for 60 hours and cooling to 0°, the title pyridinium salt was collected by filtration, washed with acetone and dried (7.4 g, 88%), m.p. 165°-170° (decomp.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04861893 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-29d7221a4db641b2bbc615bd7ea99063 |
| Source note | uspto-grants-1989_08 |