HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → HCID 14575222, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Nitrourea | HCID 62372 | — |
| Reactant | HCID 14575211 | HCID 14575211 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | 1-Propanol | HCID 1031 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 14575222 | HCID 14575222 | — |
Reaction Steps
The reaction of 3-(2,3,4,5,6-pentafluorophenoxy)-8-azabicyclo[3.2.1]octane 5 and nitrourea in an alkanol (e.g. methanol, ethanol, 1-propanol, 2-propanol, and the like; methanol being preferred) at a temperature of from about 20° C. to about 100° C., preferably from about 50° C. to about 80° C., provides a means of a furnishing an 8-aminocarbonyl-3-(2,3,4,5,6-pentafluorophenoxy)-8-azabicyclo[3.2.1]octane 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04861889 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-4ceae09f6e6b4e4585323f3187bccb58 |
| Source note | uspto-grants-1989_08 |