Hydrochloric Acid → HCID 10134275, compound

Participants

Reaction Steps

The title compound was prepared as described in Example 8 starting with (C) of Example 8 (2.0 g, 6.4 mmol) and using dipropylamine in place of dibutylamine to produce 1.2 g (40% yield) of the title compound as the HCl salt, mp 172°-173° C. IR(KBr): 3400, 1600 cm-1. MS: 379(MH+). 1H NMR (CDCl3): δ 8.48-6.95 (m, 10H), 4.19 (t, J=5.1 Hz, 2H), 3.21 (m, 6H), 2.49-0.91 (m, 12H).

Provenance & Evidence