HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18435647, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Dipropylamine | HCID 8902 | — |
| Reactant | HCID 18435640 | HCID 18435640 | — |
| Product | HCID 18435647 | HCID 18435647 | 30% |
Reaction Steps
The procedure of Example 18 was followed starting with (D) of Example 18 (2.5 g, 7.6 mmol) and using dipropylamine in place of dibutylamine to produce 0.90 g (30% yield) of the named compound as the HCl salt, mp 150°-152° C. IR(KBR): 1600 cm-1. MS: 393(MH+). 1H NMR (CDCl3): δ 8.09-6.87 (m, 10H), 4.01 (t, J=5.4 Hz, 2H), 3.02 (m, 6H), 1.95 (m, 8H), 0.99 (m, 6H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04861897 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-2ce1dd42433d4964b73bb2e8ed6ae2d6 |
| Source note | uspto-grants-1989_08 |