Hydrochloric Acid → HCID 18435654, compound

Participants

Reaction Steps

The title compound was prepared in accordance with Example 18 starting with (D) of Example 18 (2.5 g, 7.6 mmol) and using imidazole in place of dibutylamine to produce 1.1 g (40% yield) of the title compound as the HCl salt, mp 204°-205° C. IR(KBr): 3400, 1600 cm-1. MS: 360(MH+). 1H NMR (CD3OD): δ 9.02 (s, 1H), 7.89-6.89 (m, 12H), 4.38 (t, J=5.3 Hz, 2H), 4.08 (t, J=5.4 Hz, 2H), 1.97 (m, 4H).

Provenance & Evidence