Hydrochloric Acid → HCID 14146379, compound

Participants

Reaction Steps

The title compound was prepared as described in Example 28 starting with (F) of Example 28 (3.0 g, 9.8 mmol) and using diethylamine in place of dibutylamine to produce 0.81 g (24% yield) of the title compound as the HCl salt, mp 187°-188° C. IR(KBr): 3400, 1600 cm-1. MS: 367(MH+). 1H NMR (CD3OD): δ 8.22-6.99 (m, 10H), 4.21 (t, J=5.1 Hz, 2H), 3.34 (m, 6H), 2.33 (m, 2H), 1.42 (m, 6H).

Provenance & Evidence