Hydrochloric Acid → HCID 14146384, compound

Participants

Reaction Steps

The title compound was prepared in accordance with Example 28 starting with (F) of Example 28 (5.0 g, 15 mmol) and using imidazole in place of dibutylamine to produce 2.4 g (39% yield) of the title compound as the HCl salt, mp 231°-232° C. IR(KBr): 1595 cm-1. MS: 362(MH+). 1H NMR (CD3OH): δ 9.01 (s, 1H), 7.99-6.91 (m, 12H), 4.21 (t, J=5.2 Hz, 2H), 4.03 (t, J=5.3 Hz, 2H), 2.32 (m, 2H).

Provenance & Evidence