HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 10133649, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Dipropylamine | HCID 8902 | — |
| Reactant | HCID 14146396 | HCID 14146396 | — |
| Product | HCID 10133649 | HCID 10133649 | 19% |
Reaction Steps
The title compound was prepared as described in Example 43 starting with (I) of Example 43 (2.0 g, 6.3 mmol) and using dipropylamine in place of dibutylamine to produce 0.41 g (19% yield) of the title compound as the HCl salt, mp 142°-143° C. IR(KBr): 3400, 1600 cm-1. MS: 369(MH+). 1H NMR (CDCl3): δ 8.19-6.95 (m, 8H), 4.19 (t, J=5.1 Hz, 2H), 3.01 (m, 6H), 2.64-0.82 (m, 12H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04861897 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-02dffdd7c06e4f6e9e30eccb72326465 |
| Source note | uspto-grants-1989_08 |