HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isothiocyanatoformate → HCID 178473562, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isothiocyanatoformate | HCID 85320 | — |
| Reactant | Cis tert-Butyl 4-aminocyclohexylcarbamate | HCID 2756050 | — |
| Product | HCID 178473562 | HCID 178473562 | — |
Reaction Steps
To a solution of 1.10 g of (4-amino-cyclohexyl)-carbamic acid tert-butyl ester in 25 ml of EtAc 0.58 ml of ethoxycarbonyl-isothiocyanat are added and the mixture obtained is stirred at RT. The precipitate formed is filtered and washed with diethylether. [trans-4-(3-Ethoxycarbonyl-thioureido)cyclohexyl]carbamic acid tert-butyl ester is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07485632B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-3dbeb131fff14f5c8f875c9d5060d5c9 |
| Source note | uspto-grants-2009_02 |