HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178504046, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 178454037 | HCID 178454037 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178504046 | HCID 178504046 | — |
Reaction Steps
A mixture of 1.19 g of (trans-4-thioureido-cyclohexyl)-carbamic acid tert-butyl ester and 0.41 ml of methyliodide in 50 ml of MeOH is stirred at RT. From the mixture obtained solvent is evaporated and [trans-4-(2-methyl-isothioureido)-cyclohexyl]-carbamic acid tert-butyl ester in the form of a hydrolodide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07485632B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-941be3564bea4ff8bf63eedef6b4b1ab |
| Source note | uspto-grants-2009_02 |