HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → Hydrogen iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | [4-(1,3-Dimethyl-thioureido)-cyclohexyl]carbamic acid benzylester | HCID 87643180 | — |
| Solvent | 2-Oxopropiononitrile | HCID 69430 | — |
| Product | Hydrogen iodide | HCID 24841 | — |
| Product | HCID 68981797 | HCID 68981797 | — |
Reaction Steps
0.18 ml of methyliodide are added to a solution of 0.64 g [4-(1,3-dimethyl-thioureido)-cyclohexyl]carbamic acid benzylester in 30 ml of AcCN. The mixture obtained is refluxed for 2.5 hours and solvent is evaporated. [4-(1,2,3-Trimethyl-isothioureido)-cyclohexyl]-carbamic acid benzylester in the form of a hydroiodide is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07485632B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-dfa80a1a88114ecb8b1374df58ae837b |
| Source note | uspto-grants-2009_02 |