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HRID1723626

反应详情

EQUATION

反应方程式

HRID 1723626 的结构方程式

REACTANTS

反应物

2
结构：CI
HCID6328

Methyl iodide

CH3I

结构：CNC(=S)N(C)C1CCC(NC(=O)OCc2ccccc2)CC1
HCID87643180

未命名化合物

PRODUCTS

生成物

2
结构：I
HCID24841

Hydrogen iodide

HI

结构：CN=C(SC)N(C)C1CCC(NC(=O)OCc2ccccc2)CC1
HCID68981797

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)C#N
溶剂HCID69430

2-Oxopropiononitrile

C3H3NO

PROCEDURE

实验过程

0.18 ml of methyliodide are added to a solution of 0.64 g [4-(1,3-dimethyl-thioureido)-cyclohexyl]carbamic acid benzylester in 30 ml of AcCN. The mixture obtained is refluxed for 2.5 hours and solvent is evaporated. [4-(1,2,3-Trimethyl-isothioureido)-cyclohexyl]-carbamic acid benzylester in the form of a hydroiodide is obtained.

WORKUP

后处理

  1. customThe mixture obtained
  2. temperatureis refluxed for 2.5 hours
  3. customsolvent is evaporated