Isopropanol → 2-Isopropoxy-5-methylsulfonylbenzoic acid

HRID 1723647Notes

Reaction equation

HRID 1723647 reaction equation
Cl[C:2]1[CH:10]=[CH:9][C:8]([S:11]([CH3:14])(=[O:13])=[O:12])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5].[CH:15]([OH:18])([CH3:17])[CH3:16]>>[CH:15]([O:18][C:2]1[CH:10]=[CH:9][C:8]([S:11]([CH3:14])(=[O:13])=[O:12])=[CH:7][C:3]=1[C:4]([OH:6])=[O:5])([CH3:17])[CH3:16]

Participants

3

Reactant 2

HCID 3776IsopropanolHCID 23291322-Chloro-5-(methylsulphonyl)benzoic acid

Product 1

HCID 211002372-Isopropoxy-5-methylsulfonylbenzoic acid

Procedure

According to the procedure described for the synthesis of example 4, step c, the title compound has been synthesized from 2-chloro-5-methanesulfonyl-benzoic acid and isopropanol. MS (m/e): 257.0 (M−H, 100%)

Workup

  1. customdescribed for the synthesis of example 4, step c

Sources & evidence

ORD record
ord-d8c6d62b01df4eefb359fc626d7f647d
Source dataset
uspto-grants-2009_02
Patent number
US07485637B2

Reaction notes

Loading…