HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57434154, compound → HCID 68871245, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57434154 | HCID 57434154 | — |
| Reactant | HCID 68871757 | HCID 68871757 | — |
| Product | HCID 68871245 | HCID 68871245 | 23% |
Reaction Steps
3-Bromo-7-ethyl-7H-imidazo[1,2-a]pyrazin-8-one and 4-fluoro-3-(2-methyl-2H-[1,2,4]triazol-3-ylmethoxy)benzeneboronic acid were coupled to give the title compound as a white solid (43 mg, 23%): δH (400 MHz, d6-DMSO) 1.26 (3H, t, J 7), 3.94 (3H, s), 3.96 (2H, s), 5.52 (2H, s), 7.22-7.26 (2H, m), 7.44 (1H, dd, J 11 and 8), 7.65 (1H, d, J 6), 7.64 (1H, dd, J 8 and 2), 7.66 (1H, s), 7.98 (1H, s); m/z (ES+) 369 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07485640B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-be2110edb5a244d5bfe9323424d42015 |
| Source note | uspto-grants-2009_02 |