HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 57420547, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Nitrogen | HCID 947 | — |
| Reactant | tert-Butyl methyl ether | HCID 15413 | — |
| Reactant | HCID 11510935 | HCID 11510935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 57420547 | HCID 57420547 | — |
Reaction Steps
4.840 mg of concentrated hydrobromic acid was added to 0.89 ml of a solution of 1-(2-fluorophenyl)-3-(piperidin-4-yloxy)-1H-indazole in MeOH (concentration=10.3 mg/ml). The solution was placed under a stream of N2 gas until no solvent remained. Approximately 0.5 ml of MTBE was added and the sample was left open and stirred overnight. A white solid remained upon recovery.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07485636B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-10276e7162f24b6aa1b270477fd6737f |
| Source note | uspto-grants-2009_02 |