HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol, 1-bromo- → HCID 178480899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol, 1-bromo- | HCID 14202443 | — |
| Reactant | (E)-3-methyl-N-[(1-methylimidazol-2-yl)methylideneamino]-1,3-benzothiazol-2-imine | HCID 87882107 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178480899 | HCID 178480899 | — |
Reaction Steps
1.00 g (3.68 mmol) of 1-methyl-1H-imidazol-2-carboxaldehyde [(2E)-3-methyl-1,3-benzothiazol-2(3H)-ylidene] hydrazone from Step 1 and 0.69 g (5.52 mmol) of bromoethanol in acetonitrile were heated at reflux for 2 hours. After the solvent was removed, the precipitate formed was suction-filtered off, washed with ethyl acetate and dried under vacuum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07488353B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-bbd8fc960495476d8ef6e1a1b41ce03d |
| Source note | uspto-grants-2009_02 |