HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 86023618, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 86606190 | HCID 86606190 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86023618 | HCID 86023618 | — |
Reaction Steps
Hydrazine monohydrate was added to a methylene chloride solution of diethyl [2-(1,3-dioxo-1,3-dihydro-2H-isoindol-2-yl)-1,1-difluoroethyl]phosphonate, for stirring at ambient temperature for one hour, to obtain diethyl (2-amino-1,1-difluoroethyl)phosphonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07488739B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-efdd873ef6424f818e22ca9528e71845 |
| Source note | uspto-grants-2009_02 |