HCID 57561099, compound → HCID 57561143, compound

Participants

Reaction Steps

6-Methoxymethyl-3-nitro-pyridine-2,4-diamine (455 mg, 2.29 mmol) is dissolved in EtOH (50 mL) and 10% Pd/C (50 mg) is added. The mixture is hydrogenated at 50 psi for 2 hours. The reaction mixture is filtered through Celite and the Celite bed washed with EtOH (25 mL). The solvent is removed under reduced pressure to yield the title compound as an off-white solid.

Provenance & Evidence