HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium formate → HCID 46203238, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium formate | HCID 2723923 | — |
| Reactant | HCID 46203237 | HCID 46203237 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 46203238 | HCID 46203238 | — |
Reaction Steps
Stir a mixture of 2-chloro-4-methoxy-7-[3-(trifluoromethyl)pyridin-2-yl]quinoline (111 mg), ammonium formate (190 mg), 10% palladium on carbon (30 mg) in methanol (10 mL) at room temperature for 2 hours. Cool, filter through Celite and evaporate to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07488740B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-fbfa73388a504b9697dcc56d29e9b50a |
| Source note | uspto-grants-2009_02 |