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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1725164Generated: November 3, 2026

Triethylamine → HCID 57423682, compound

https://huagongshe.com/reaction/1725164

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
Reactant5-Methylisoxazole-3-carbonyl chlorideHCID 2736894—
ReactantHCID 57423680HCID 57423680—
SolventDichloromethaneHCID 6344—
ProductHCID 57423682HCID 57423682—

Reaction Steps

To a solution of [2-(3-amino-phenyl)-5-phenyl-pyrrol-1-yl]-acetic acid methyl ester (0.1 mmol) in DCM (2 mL) is added 5-methyl-isoxazole-3-carbonyl chloride (0.1 mmol) and triethylamine (0.02 mmol). The reactions are agitated at room temperature over night. The solvent is removed under vacuum and the residues are subsequently dried under high vacuum at 50° C. for 2 h.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07488832B2
Source datasetuspto-grants-2009_02
ORD IDord-c2ff7bb72bc24bd1baf804dccfeef0e6
Source noteuspto-grants-2009_02