HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 57423682, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 5-Methylisoxazole-3-carbonyl chloride | HCID 2736894 | — |
| Reactant | HCID 57423680 | HCID 57423680 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57423682 | HCID 57423682 | — |
Reaction Steps
To a solution of [2-(3-amino-phenyl)-5-phenyl-pyrrol-1-yl]-acetic acid methyl ester (0.1 mmol) in DCM (2 mL) is added 5-methyl-isoxazole-3-carbonyl chloride (0.1 mmol) and triethylamine (0.02 mmol). The reactions are agitated at room temperature over night. The solvent is removed under vacuum and the residues are subsequently dried under high vacuum at 50° C. for 2 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07488832B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-c2ff7bb72bc24bd1baf804dccfeef0e6 |
| Source note | uspto-grants-2009_02 |