HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 19593566, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 9-Acetyl-9H-carbazole | HCID 95837 | — |
| Reactant | 3,6-Dichlorocarbazole | HCID 236487 | — |
| Reactant | Sodium Methoxide | HCID 10942334 | — |
| Product | HCID 19593566 | HCID 19593566 | — |
Reaction Steps
Reaction of 2-coumarine (CAS 553-86-6) with methyl(triphenylphosphoranylidene)acetate (CAS 2605-67-6) gives compound 1 (Aust. J. Chem., 1975, 28, 1097). Reaction of compound 1 with acetyl chloride (CAS 75-36-5) leads to compound 2 (J. Chem. Soc., Perkin Trans 1, 1984, 1605). Reaction of compound 2 with sodium methylate affords dibenzo[b,d]furan-1,3-diol 1-2 (J. Chem. Soc., Perkin Trans 1, 1984, 1605).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07491245B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-e8678f9849f348a7bc16dbb53b32e52e |
| Source note | uspto-grants-2009_02 |