Lithium Hydroxide → HCID 68862480, compound

Participants

Reaction Steps

A mixture of Example 575A and Example 576A (0.10 g) was treated with LiOH according to the procedure of Example 385I, giving the title compound, 12.4 mg, and Example 576B, 42 mg. 1H NMR (DMSO-d6) δ 1.06 (t, 3H), 2.42 (q, 2H), 2.84 (t, 2H), 3.15 (t, 2H), 3.62 (s, 3H), 6.74 (d, 1H), 7.18-7.22 (m, 2H), 7.14-7.30 (m, 4H), 7.35 (t, 1H), 7.45 (d, 1H), 7.55 (t, 1H), 7.80 (d, 1H), 9.95 (s, 1H), 13.20 (br s, 1H); MS (ESI(−)) m/e 438 (M−H)−.

Provenance & Evidence