HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl 4-oxopiperidine-1-carboxylate → HCID 68972754, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl 4-oxopiperidine-1-carboxylate | HCID 735900 | — |
| Reactant | 4-(Methylsulfonyl)aniline hydrochloride | HCID 2735180 | — |
| Product | HCID 68972754 | HCID 68972754 | 50% |
Reaction Steps
Using general procedure A, 1-Boc-4-piperidone (2.01 g, 10.09 mmol) and 4-(methanesulfonyl)aniline hydrochloride (1.69 g, 8.13 mmol) afforded 4-(4-methanesulfonyl-phenylamino)-piperidine-1-carboxylic acid tert-butyl ester as a white solid (1.44 g, 50%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07491735B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-42b7b0decc7b4b52982b46bf9fd32b9e |
| Source note | uspto-grants-2009_02 |