1-Phenyl-1-cyclopentanol → Benzene, 1-cyclopenten-1-yl-

HRID 1726850ノート

反応式

HRID 1726850 の反応式
O[C:2]1([C:7]2[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=2)[CH2:6][CH2:5][CH2:4][CH2:3]1>C1COCC1>[C:7]1([C:2]2[CH2:6][CH2:5][CH2:4][CH:3]=2)[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1

参加物

3

反応物 1

HCID 1391651-Phenyl-1-cyclopentanol

生成物 1

HCID 136652Benzene, 1-cyclopenten-1-yl-収率 85%

試薬・触媒・溶媒 1

HCID 8028Tetrahydrofuran溶媒

実験手順

The same experiment as in Example 3 was carried out, except for using 50 ml of THF instead of 50 ml of CPME. The resulting reaction mixture was analyzed by gas chromatography to confirm that the target 1-hydroxy-1-phenylcyclopentane and phenylcyclopentene were obtained in a yield of 85% in total.

後処理

  1. customThe resulting reaction mixture

出典と根拠

ORDレコード
ord-096630f9002949e8adfacd8577ddf798
出典データセット
uspto-grants-2009_02
特許番号
US07494962B2

反応ノート

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