HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 69053917, compound → HCID 69060894, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 69053917 | HCID 69053917 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 69060894 | HCID 69060894 | — |
Reaction Steps
1-(Phenylmethyl)piperidin-4-yl butylcarbamate (Preparation 109, 13.0 g) in ethanol (100 ml) containing palladium (5% on carbon) was hydrogenated at 60 psi to give the title compound as a green oil that solidified upon standing.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07494992B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-cc394d9de4564166b92d281de96e1a5d |
| Source note | uspto-grants-2009_02 |