HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Dihydroxy-3-allylbenzophenone → (2,4-Dihydroxy-3-propylphenyl)(phenyl)methanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Dihydroxy-3-allylbenzophenone | HCID 21910981 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | (2,4-Dihydroxy-3-propylphenyl)(phenyl)methanone | HCID 13019373 | — |
Reaction Steps
A solution of 2,4-dihydroxy-3-(2-propenyl)benzophenone (3 g) was reduced under ˜1 atm H2 in ethyl acetate (100 mL) over 10% Pd/C catalyst (0.3 grams) for 3 hours. The product was purified by crystallization from methanol/water. The product is obtained as small yellow plates.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07495020B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-de268f8f414d4757a863a9b72dc3d063 |
| Source note | uspto-grants-2009_02 |