HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzeneacetic acid, alpha-bromo-, methyl ester → HCID 21985926, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzeneacetic acid, alpha-bromo-, methyl ester | HCID 137806 | — |
| Reactant | HCID 135723523 | HCID 135723523 | — |
| Product | HCID 21985926 | HCID 21985926 | — |
Reaction Steps
The phenol of step 1 (0.25 g, 0.86 mmol) was coupled with commercially available methyl 2-bromo-2-phenylacetate (0.20 g, 0.86 mmol) as was described for example 9, step 5. The product was purified by chromatography on silica gel eluting with ethyl acetate:hexane (10:90).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07495020B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-8cfecc54c15b4c01a73d6dcc68127bd9 |
| Source note | uspto-grants-2009_02 |