HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Dipropylphenol → 2,6-Dipropyl4-propionylphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Dipropylphenol | HCID 81107 | — |
| Reactant | Sodium Propionate | HCID 2723816 | — |
| Solvent | Trifluoromethanesulfonic acid | HCID 62406 | — |
| Product | 2,6-Dipropyl4-propionylphenol | HCID 11310872 | — |
Reaction Steps
Sodium propanoate (0.88 g, 1.5 eq) and 2,6-dipropylphenol (1.09 g, 1.0 eq) were combined in Triflic Acid (5.0 g) as in Example 13, step 1. The resulting waxy solid was purified by chromatography on silica gel using ethyl acetate:hexanes:acetic acid (10:90:1) to give the titled phenol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07495020B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-3b0334179b264f1582ed15228403292d |
| Source note | uspto-grants-2009_02 |