HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Hydroxide → HCID 23704465, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 21082128 | HCID 21082128 | — |
| Solvent | Methanol--water (1/1) | HCID 22242641 | — |
| Product | HCID 23704465 | HCID 23704465 | 125.1% |
Reaction Steps
Part A: A mixture of ethyl 1-(4-chlorophenyl)-2-(2,4-dichlorophenyl)-4,5-dihydro-1H-imidazole-4-carboxylate (3.97 g, 0.01 mol) in methanol/water is reacted with LiOH (1.3 gram, 0.054 mol) at room temperature for 16 hours. The resulting mixture is concentrated in vacuo to give crude lithium 1-(4-chlorophenyl)-2-(2,4-dichlorophenyl)-4,5-dihydro-1H-imidazole-4-carboxylate (4.7 gram).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07495108B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-c54492847b7e45ae9512c523d155bff0 |
| Source note | uspto-grants-2009_02 |