HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 10117784, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | HCID 9827369 | HCID 9827369 | — |
| Reactant | Ammonium cerium-nitrate | HCID 57418452 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 10117784 | HCID 10117784 | — |
Reaction Steps
2 ml of acetone was added to 50.7 mg (0.100 mmol) of 4-(3-chlorophenyl)-2,6-dimethyl-1,4-dihydropyridine-3,5-dicarboxylic acid mono (3,3-diphenylpropyl) ester. 130 mg (0.240 mmol) of cerium ammonium nitrate suspended in 1 ml of water was added and stirred at room temperature for 10 minutes. After adding water and extracting with ethyl acetate, the organic layer was dried over anhydrous sodium sulfate and then concentrated under reduced pressure to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07494989B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-4033948ededf4d12a051f34494313dcd |
| Source note | uspto-grants-2009_02 |