HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 69063286, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 69074752 | HCID 69074752 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | HCID 178418361 | HCID 178418361 | — |
| Product | HCID 69063286 | HCID 69063286 | — |
Reaction Steps
5 ml of ethyl acetate and 10% palladium carbon were added to 340 mg (0.640 mmol) of 2-(2-chloroethoxy) methyl-4-(3-chlorophenyl)-6-methyl-1,4-dihydropyridine-3,5-dicarboxylic acid 3-benzyl ester 5-(2-cyanoethyl) ester. The obtained solution was stirred at room temperature in hydrogen atmosphere under normal pressure for 8 hours. After filtering the reaction mixture, the filtrate was evaporated under reduced pressure to obtain the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07494989B2 |
| Source dataset | uspto-grants-2009_02 |
| ORD ID | ord-a029e48d196141d39b0646b54456613b |
| Source note | uspto-grants-2009_02 |