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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1727909Generated: November 1, 2026

Ethyl Acetate → HCID 69063286, compound

https://huagongshe.com/reaction/1727909

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthyl AcetateHCID 8857—
ReactantHCID 69074752HCID 69074752—
CatalystHCID 178418390HCID 178418390—
SolventHCID 178418361HCID 178418361—
ProductHCID 69063286HCID 69063286—

Reaction Steps

5 ml of ethyl acetate and 10% palladium carbon were added to 340 mg (0.640 mmol) of 2-(2-chloroethoxy) methyl-4-(3-chlorophenyl)-6-methyl-1,4-dihydropyridine-3,5-dicarboxylic acid 3-benzyl ester 5-(2-cyanoethyl) ester. The obtained solution was stirred at room temperature in hydrogen atmosphere under normal pressure for 8 hours. After filtering the reaction mixture, the filtrate was evaporated under reduced pressure to obtain the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07494989B2
Source datasetuspto-grants-2009_02
ORD IDord-a029e48d196141d39b0646b54456613b
Source noteuspto-grants-2009_02