HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → 5-Ethoxypyrimidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | 2-[4-(3-Acetoxy-1-butenyl)phenyl]-5-ethoxypyrimidine | HCID 53899234 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 5-Ethoxypyrimidine | HCID 19921688 | — |
Reaction Steps
9 g of 2-[4-(3-acetoxy-1-butenyl)phenyl]-5-ethoxypyrimidine, 2 g of palladium on active charcoal (10 wt. %) and 150 ml of tetrahydrofuran were hydrogenated in an analogous manner to Example 1(e) to give 8.2 g of 2-(3-acetoxy-1-butyl)phenyl]-5-(ethoxy)pyrimidine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05326497 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-722e6aca303a45a698cae6c0b9f8ad49 |
| Source note | uspto-grants-1994_07 |