HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methane → HCID 19017137, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | 5-Trimethylsilyloxy-2-(4-[5-hydroxy-1-pentenyl]phenyl)pyridine | HCID 54318196 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 19017137 | HCID 19017137 | 93.9% |
Reaction Steps
5.4 g of 5-trimethylsilyloxy-2-(4-[5-hydroxy-1-pentenyl]phenyl)pyridine, 1 g of palladium on active charcoal (10 w/w %) and 50 ml of ethyl acetate were reacted in an analogous manner to Example 1(c) to give 5.1 g of 5-trimethylsilyloxy-2-(4-[5-hydroxy-1-pentyl]phenyl)pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05326497 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-f7448474334b45799f63380712f00ea3 |
| Source note | uspto-grants-1994_07 |