HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 67635417, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | ethyl N-ethoxycarbonyliminocarbamate | HCID 220568 | — |
| Reactant | 3-Octen-1-ol, (3Z)- | HCID 5364519 | — |
| Reactant | 2-[4-(5-[Propyloxy]-1-pentyl)phenyl]-5-hydroxypyridine | HCID 19017092 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67635417 | HCID 67635417 | 59.6% |
Reaction Steps
1.0 g of 2-[4-(5-[propyloxy]-1-pentyl)phenyl]-5-hydroxypyridine, 0.42 g of (Z)-3-octen-1-ol, 0.58 g of diethyl azodicarboxylate, 0.88 g of triphenylphosphine and 100 ml of tetrahydrofuran are reacted in an analogous manner to Example 3 to give 0.8 g of 2-[4-(5-[propyloxy]-1-pentyl)phenyl]-5-([(Z)-3-octenyl]oxy)pyridine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05326497 |
| Source dataset | uspto-grants-1994_07 |
| ORD ID | ord-5146ff67b9244daa917fa13402352325 |
| Source note | uspto-grants-1994_07 |